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Table 4 Predicted compositions of glycan chains in isolated stingray GRLN-LP

From: Ghrelin-like peptide with fatty acid modification and O-glycosylation in the red stingray, Dasyatis akajei

Peak

Mass [M+H]+

Possible compositions of glycan chains

Remarks

1

2580.15

Thr-11+(HexNAc)3(Hex)

Single peak

2

3351.68

Ser-10+(HexNAc)3(Hex)

m/z 2580.14 was detected

  

Thr-11+(HexNAc)3(Hex)

 
 

3513.74

Ser-10+(HexNAc)3(Hex)

m/z 2580.14 was detected

  

Thr-11+(HexNAc)3(Hex)2

 

3

3375.42

Ser-10+(HexNAc)3(Hex)

m/z 24 adduct of peak 2

  

Thr-11+(HexNAc)3(Hex)

 
 

3537.46

Ser-10+(HexNAc)3(Hex)

m/z 24 adduct of peak 2

  

Thr-11+(HexNAc)3(Hex)2

 

4

2580.26

Thr-11+(HexNAc)3(Hex)

 
 

2742.33

Thr-11+(HexNAc)3(Hex)2

 

5, 6

2604.15

Thr-11+(HexNAc)3(Hex)

m/z 24 adduct of peak 1

 

2766.20

Thr-11+(HexNAc)3(Hex)2

m/z 24 adduct of peak 1

7

2594.15

Thr-11+(HexNAc)3(Hex)

m/z 14 adduct of peak 4

 

2756.21

Thr-11+(HexNAc)3(Hex)2

m/z 14 adduct of peak 4